10.1 Introduction. This section describes field instruments commonly used in inspection of field painting. The References section of this handbook lists the full title and sources of standard test methods referenced in this section. For equipment descriptions having no referenced standards, no standards are available. Typical suppliers include:

a) Paul N. Gardner Company, Inc., Gardner Building, P. O. Box 10688, Pompano Beach, FL 33060-6688.

b) KTA-TATOR, Inc., 115 Technology Drive, Pittsburgh,

PA 15275.

c) ZORELCO, P. O. Box 25500, Cleveland, OH 44125.

d) Pacific Scientific, 2431 Linden Lane, Silver Spring, MD 20910.

e) S. G. Pinney & Associates, 2500 S. E. Midport Road, P. O. Box 9220, Port St. Luice, FL 34952.

10.2 Illuminated Microscope. A pocket-sized illuminated microscope is frequently used to detect mill scale, other surface contamination, pinholes, fine blisters, and other microscopic conditions during painting operations. These microscopes are available with magnifications of 5 and higher.

10.3 Instruments for Use With Abrasive Blasting. A few instruments are available for testing the operational readiness of equipment for abrasive blasting of metals for painting.

10.3.1 Gage for Determining Nozzle Pressure. A pocket-sized pressure gage with a hypodermic needle is used to determine the blasting pressure at the nozzle. The needle is inserted in the blasting hose just before the nozzle in the direction of the flow. Instant readings can be made up to 160 pounds per square inch (gage) (psig).

10.3.2 Wedge for Determining Diameter of Nozzle Orifice. A hand-held calibrated wedge is inserted in the direction of flow into the nozzle orifice to determine its size (inches) and airflow (cfm at 100 psig). The orifice measuring range is 1/4 to 5/8 inch, and the airflow range is 81 to 548 cfm.

10.3.3 Surface Contamination Detection Kit. The level of cleanliness of abrasive blast cleaned steel can be determined by comparing it with SSPC VIS 1 photographic standards. SSPC VIS 3 photographic standards are used for determining level of

cleanliness of hand-cleaned steel and power-tool cleaned steel. Standard coupons of steel blasted to different levels of cleanliness are also available for comparison from NACE, and procedures for their use are given in NACE TM0170. Test kits for detection of chloride, sulfate, and ferrous ions, as well as pH, are commercially available. They contain strips, swabs, papers, and operating instructions for simple chemical testing.

10.3.4 Profile of Blasted Steel. There are three methods for determining the profile (maximum peak-to-valley height) of blasted steel surfaces described in ASTM D 4417. Comparators. Several types of comparators are available for determining surface profile. These include ISO, Clemtex, and Keene-Tator comparators. Basically, they use a 5-power illuminated magnifier to permit visual comparison of the blast-cleaned surface to standard profile depths. Standards are available for sand, grit, and shot-blasted steel. Surface Profile Gages. A surface profile gage is an easy instrument to use to determine surface profile, but 10 to 20 measurements must be averaged to obtain reliable results. The gage consists of an instrument with a flat base that rests on the profile peaks and a tip that projects into the valleys. The tip can be blunted by dragging it across steel surfaces. This prevents the tip from reaching the bottom of the valleys in the profile, resulting in a profile value that is less than the correct value. Testex Press-O-Film Replicate Tape. Testex Press-O-Film replicate tape produces the most precise profile measurements, according to the precision statement of ASTM D 4417. The tape consists of a layer of deformable plastic bonded to a polyester backing. The tape is rubbed onto the blast – cleaned surface with a plastic swizzle stick to produce a reverse replicate of the profile. The tape profile is then measured with a spring micrometer. The micrometer can be set to automatically subtract the 2-mil non-deformable polyester backing. After measurements, the tapes can be stored as records of profile heights.

10.3.5 Thermometers. Several different types of thermometer and temperature recorders are available for field use. They are used to measure ambient temperatures, surface temperatures of steel, and temperatures of wet paints.

10.3.6 Psychrometers. Several different manual or battery – powered psychrometers are available for measuring air temperatures, relative humidity, and dew point. In most cases, two glass thermometers are used with the instrument, as described in ASTM E 667, Clinical Thermometers (Maximum Self-Registering, Mercury-in-Glass). One thermometer has a clean "sock" or "wick" on it that is wetted with water. Air is circulated around the thermometers by the motorized fan or by whirling the hand-held sling psychrometer. Whirling should be with a steady, medium speed. Both thermometers should be read periodically and the airflow (whirling) continued until the reading becomes constant.

The "wet" bulb thermometer temperature will be lowered by evaporation of the water on the sock. The evaporation rate is related to the relative humidity and barometric pressure. Psychrometric tables relate temperature depression (difference between "dry" and "wet" bulb readings) to relative humidity and dew point. These standard tables, available from suppliers of psychrometers, cover the range from 23.0 to 30.0 inches barometric pressure. The effect of barometric pressure is relatively small; if it is unknown, use the 30.0-inch pressure table near sea level and the 29.0-inch pressure table at high elevations.

10.3.7 Wind Meter. A pocket-size wind meter is available for determining wind speed in miles per hour and velocity of air moving across a spray booth. Spraying on days with excessive winds can cause overspray or dry spray problems.

10.3.8 Moisture Meter. Meters are available for determining the moisture content of wood, plaster, concrete, or other materials. Some are nondestructive, while others require contact pins to be driven into the surface. An alternate non-destructive procedure for determining if too much moisture is present in cementitious surfaces is described in ASTM D 4263.

10.3.9 Wet Film Gage. Gages for determining paint wet film thickness are available in different types, two of which are described in ASTM D 1212 and one in ASTM D 4414. All are destructive in that they disturb the paint and require touching up the film. Notched Metal Gage. The most widely used type of wet film thickness gage, described in ASTM D 4414, consists of a thin rigid metal notched gage, usually with four working faces. Each of the notches in each working face is cut progressively deeper in graduated steps. The gage with the scale that encompasses the specified thickness is selected for use. To conduct the measurement, the face is pressed firmly and squarely into the wet paint immediately after its application. The face is then carefully removed and examined visually. The wet film thickness is the highest scale reading of the notches with paint adhering to it. Measurements should be made in triplicate. Faces of gages should be kept clean by removing the wet paint immediately

after each measurement. An alternative circularly notched gage ("hot cake") is rolled perpendicularly through the wet film and the clearance of the deepest face wetted is noted. Cylindrical Gage. A cylindrical wet film thickness gage is described in ASTM D 1212. These gages are also rolled through the paint rather than being pressed into it. They have an eccentric center wheel with constantly changing clearance supported by two outer wheels. The position on the exterior scale corresponding to the point that the wet paint first touches the eccentric wheel indicates the wet film thickness.

10.3.10 Dry Film Thickness Gages for Coatings on Aluminum, Copper, and Stainless Steel. Gages are available to determine the dry film thickness of organic coatings on aluminum, copper, and stainless steel. Alternating current from the instrument probe coil induces eddy currents in the metal that in turn induce magnetic fields that modify the electrical characteristics of the coil. ASTM D 1400 fully describes the instrument and its operating procedure.

10.3.11 Magnetic Dry Film Thickness Gages for Coatings on Steel. There are many different types of gages available for nondestructively determining the film thickness of cured organic coatings on metal surfaces. Most rely on the ferromagnetic properties of steel. Their use is described in detail in ASTM D 1186 and SSPC PA 2. They are available in different thickness ranges to provide the best accuracy with different coating thicknesses. Each has a probe or tip that is placed directly on the coating during measurement.

a) Magnetic thickness gages should be calibrated before use. It is also a good practice to check the calibration during and after use. Gage suppliers provide a set of standard thickness nonmagnetic (plastic or nonferrous metal) shims to cover their working ranges. The shim for instrument calibration should be selected to match the expected coating thickness. It is placed on a bare steel surface and the gage probe placed on it for calibration. If the instrument scale does not agree with the shim, it should be properly adjusted. If adjustment is difficult, the reading for bare steel can be added or subtracted from field readings to determine actual thicknesses.

b) The steel surface used for calibration should be a masked-off area of the steel being painted or an unpainted reference panel of similar steel, if possible. Pull-off gages are best calibrated using small chrome-plated steel panels of precise thickness (Standard Reference Material No. 1358,

Certified Coating Thickness Calibration Standard) available from the National Institute of Standards and Technology (formerly the

National Bureau of Standards), Gaithersburg, MD 20899. These panels should not be used on magnetic flux gages, because the mass of steel is insufficient for their proper operation. Shims from pull-off gages should not be interchanged with those from magnetic flux gages.

c) About five field measurements should be made for every 100 square feet of painted surface. Each of these five measurements should be an average of three separate gage readings taken within an inch or two of each other. Measurements should be made at least 1 inch away from edges and corners. Pull-Off Gages. Pull-off gages measure film thickness by stretching a calibrated spring to determine the force required to pull an attached permanent magnet from a coated steel surface. The simplest type of pull-off instrument is the pencil gage with a coil spring attached to the magnet. It is held in a vertical position on the coated steel and lifted away slowly until the magnet pops off the surface. The paint thickness is indicated by the position of the indicator on the calibrated scale. The attractive force of the magnet varies inversely with the paint thickness.

Banana gages (long, narrow instruments) represent another form of pull-off gage. They are more versatile and precise than pencil gages. A helical spring is stretched by manually turning a graduated dial, and a pin pops up when the magnet is lifted. At least one company sells an automatic gage with a dial that turns and stops automatically. Cheaper models have a rubber foot contact for the painted surface. More expensive models have a more durable tungsten carbide foot for greater durability and precision. "V" grooves are cut in the probe housing of these gages and the electrically operated flux gages described below to permit more accurate measurement of paint dry film thicknesses on cylindrical surfaces. Flux Gages. Magnetic flux gages measure changes in the magnetic flux within the probe or the instrument itself. Flux changes vary inversely with distance between the probe and the steel. Mechanically operated instruments of this type have a horseshoe magnet that is placed directly on the coating, and readings are made from the position of a needle on a calibrated scale.

Electrically operated magnetic flux instruments have a separate instrument probe that houses the magnet. Thickness measurements are presented in a digital read-out. Some of these gages have a probe attached to the instrument to permit greater accessibility, especially in laboratory work. They may also have

attachments for strip recorders for repetitive work or alarms to produce sounds if minimum thicknesses are not met. For the paint inspector, these more sophisticated attachments are normally unnecessary.

10.3.12 Destructive (Nonmagnetic) Dry Film Thickness Gage.

There are several models of Tooke gage described in ASTM D 4138, Measurement of Dry Film Thickness of Protective Coating Systems by Destructive Means that measure paint dry film thickness on any surface by microscopic observations of precision-cut angular grooves in the film. The gage is not recommended with very soft or brittle films which distort or crumble, respectively, when cut.

A dark, thick line is first drawn on the painted surface for later reference under the magnifier. A groove is then firmly cut perpendicular across the line with a tungsten carbide cutter tip as it forms a tripod with two support legs.

The width of the cut is determined visually using the illuminated magnifier portion of the instrument. Tips with three different cutting angles are available for use with films of thickness up to 50 mils. Visual observations are multiplied by 1, 2, or 10, depending upon the cutting angle of the tip, to determine the actual film thickness. Thicknesses of individual coats of a multi-coat system can be determined, if they are differently colored.

10.3.13 Holiday Detector. Instruments for detecting pinholes and other flaws in coatings on metal surfaces are used mostly on waterfront and fuel storage and distribution facilities but should be used on freshly coated critical metal structures. Holiday detectors are available in two types: low and high

voltage, as described in NACE RP0188. Low Voltage Holiday Detectors. Low voltage (30 to 90 volts) detectors are used on coatings up to 20 mils in thickness. These portable devices have a power source (a battery), an exploring electrode (a dampened cellulose sponge), an alarm, and a lead wire with connections to join the instrument to bare metal on the coated structure. A wetting agent that evaporates upon drying should be used to wet the sponge for coatings greater than 10 mils in thickness. The wetted sponge is slowly moved across the coated surface so that the response time is not exceeded.

When a holiday is touched, an electric circuit is completed through the coated metal and connected wire back to the instrument to sound the alarm. Holidays should be marked after detection for repair and subsequent retesting. High Voltage Holiday Detectors. High voltage (up to 30,000 volts or more) holiday detectors are normally used on coatings greater than 20 mils in thickness. The rule of thumb is to use 100 volts per mil of coating. The exploring electrode may consist of a conductive brush or coil spring. It should be moved at a rate not to exceed the pulse rate of the detector. If a holiday or thin spot in the coating is detected, a spark will jump from the electrode through the air space or a thin area of the coating to the metal. The resultant hole in the coating will locate the holiday or thin spot that requires corrective action.

10.3.14 Adhesion Tester. There are two basic types of testing for determining adhesion of coatings: the tape and the pull-off

test. The tape test is mostly used in the field, and the pull – off test, in the laboratory. The tape test is most useful when adhesion is low. Thus, it is often used to determine whether an old coating has adequate adhesion to support another layer of paint, or whether there is compatibility between coating layers. This test cannot distinguish among good adhesion levels. The pull-off test is more time consuming to perform since a "dolly" or fixture must be glued to the surface of the coating. The test measures the tensile force needed to remove the fixture. Pull – off forces up to several thousand pounds per square inch can be measured. Tape Adhesion Test. In the tape test, ASTM D 3359, an X or a lattice pattern is cut through the coating to the substrate. Special pressure-sensitive tape is applied over the cut and rapidly pulled off at an angle of 180 degrees. The cut area is then examined for extent of deterioration. A kit is available with a knife, chrome-plated steel template and tape for performing the test. Pull-Off Adhesion Test. In the pull-off test, ASTM D 4541, a metal dolly is bonded to a coated surface at a perpendicular angle with an adhesive, usually a two-component epoxy. After the adhesive has fully cured, a force is gradually and uniformly applied to the dolly until it is detached from the coating (or until the desired pull-off level is reached). One type of pull-off tester has a hand wheel that is turned to apply the force. The hand wheel/ratchet spanner is tightened until the dolly is detached or a prescribed force is applied. Another type applies the pull force pneumatically with compressed gas.

Machine application of pull produces more accurate results than manual application. In both cases, care must be taken to make sure the dolly and instrument are both aligned perpendicular to the coated surface. A horizontal surface is preferred.

10.3.15 Portable Glossmeter. Battery-powered, pocket-size gloss meters can provide accurate measurements in the laboratory or field. ASTM D 523, Specular Gloss, describes a method for measuring gloss in the laboratory which could be adapted for use with a portable device. Measurements can be made on any plane surfaces.

10.3.16 Hardness Tester. A series of hardness pencils (drawing leads) are available for determining rigidity or hardness of organic coatings on rigid substrates. The film hardness is that of the hardest lead that does not cause damage, as described in ASTM D 3363, Film Hardness by Pencil Test. The procedure is used to establish degree of cure, adverse effects of solvents from a wet layer upon a dry film, and softening effects caused by environmental exposure.

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